Information card for entry 4115093

Structure parameters

• Formula: K6 Na6 O92 Sb2 W18 Zn3
• Calculated formula: K6 Na6 O92 Sb2 W18 Zn3
• Title of publication: Structure and Properties of the Dendron-Encapsulated Polyoxometalate (C52H60NO12)12[(Mn(H2O))3(SbW9O33)2], a First Generation Dendrizyme
• Authors of publication: Dirk Volkmer; Björn Bredenkötter; Jörg Tellenbröker; Paul Kögerler; Dirk G. Kurth; Pit Lehmann; Heimo Schnablegger; Dietmar Schwahn; Markus Piepenbrink; Bernt Krebs
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 10489 - 10496
• a: 15.265 ± 0.002 Å
• b: 15.265 ± 0.002 Å
• c: 24.461 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4936.3 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 194
• Hermann-Mauguin space group symbol: P 63/m m c
• Hall space group symbol: -P 6c 2c
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1278
• Weighted residual factors for all reflections included in the refinement: 0.1294
• Goodness-of-fit parameter for all reflections included in the refinement: 1.227
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No