Information card for entry 4115484

Structure parameters

• Chemical name: K(K-crypt)5[Bi3Cr2(CO)6]2*3en
• Formula: C106 H196 Bi6 Cr4 K6 N14 O42
• Calculated formula: C106 H196.02 Bi6 Cr4 K6 N14 O42
• Title of publication: Stabilization of Ozone-like [Bi3]3- in the Heteroatomic closo-Clusters [Bi3Cr2(CO)6]3- and [Bi3Mo2(CO)6]3-
• Authors of publication: Li Xu; Angel Ugrinov; Slavi C. Sevov
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 4091 - 4092
• a: 12.679 ± 0.003 Å
• b: 17.724 ± 0.002 Å
• c: 18.254 ± 0.002 Å
• α: 71.31 ± 0.01°
• β: 81.37 ± 0.03°
• γ: 78.82 ± 0.02°
• Cell volume: 3794.9 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1899
• Residual factor for significantly intense reflections: 0.0765
• Weighted residual factors for significantly intense reflections: 0.1665
• Weighted residual factors for all reflections included in the refinement: 0.2175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No