Information card for entry 4115965

Structure parameters

• Formula: C24 H44 La N Si3
• Calculated formula: C24 H44 La N Si3
• SMILES: [La]123456789(N([SiH](C)C)[SiH](C)C)[c]%10([Si](C)(C)[c]%117[c]8([c]9([c]1([c]%112C)C)C)C)[c]3([c]4([c]5([c]6%10C)C)C)C
• Title of publication: C2-Symmetric ansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity
• Authors of publication: Jörg Eppinger; Michael Spiegler; Wolfgang Hieringer; Wolfgang A. Herrmann; Reiner Anwander
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2000
• Journal volume: 122
• Pages of publication: 3080 - 3096
• a: 9.529 ± 0.001 Å
• b: 11.145 ± 0.001 Å
• c: 13.573 ± 0.001 Å
• α: 79.68 ± 0.01°
• β: 83.26 ± 0.01°
• γ: 77.61 ± 0.01°
• Cell volume: 1380.4 ± 0.2 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0594
• Weighted residual factors for all reflections included in the refinement: 0.0605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No