Information card for entry 4116557

Structure parameters

• Formula: C66 H66 Au4 F12 O2 P6 S2
• Calculated formula: C66 H66 Au4 F12 O2 P6 S2
• Title of publication: Electrochemical and Chemical Oxidation of Gold(I) Thiolate Phosphine Complexes: Formation of Gold Clusters and Disulfide
• Authors of publication: Jinhua Chen; Tong Jiang; Gang Wei; Ahmed A. Mohamed; Craig Homrighausen; Jeanette A. Krause Bauer; Alice E. Bruce; Mitchell R. M. Bruce
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 9225 - 9226
• a: 14.0845 ± 0.0003 Å
• b: 13.2873 ± 0.0002 Å
• c: 19.6109 ± 0.0003 Å
• α: 90°
• β: 97.516 ± 0.001°
• γ: 90°
• Cell volume: 3638.55 ± 0.11 ų
• Cell temperature: 270 ± 2 K
• Ambient diffraction temperature: 270 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0999
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for all reflections: 0.1476
• Weighted residual factors for significantly intense reflections: 0.1277
• Goodness-of-fit parameter for all reflections: 1.002
• Goodness-of-fit parameter for significantly intense reflections: 1.135
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No