Information card for entry 4116559

Structure parameters

• Chemical name: {4,4',4"-[nitrilotris-[2,1-ethanediyl(N-methylcarboxamido)]]tris[2-(6-N,N diethylcarboxamidopyridine)]} Europium(III) tris(trifluoromethanesulfonate)- hexafluorophosphate hemi acetonitrile.
• Formula: C46 H62.5 Eu F15 N10.5 O15 P S3
• Calculated formula: C46 H61 Eu F15.001 N10.5 O15 P S3
• Title of publication: Nine-Coordinate Lanthanide Podates with Predetermined Structural and Electronic Properties: Facial Organization of Unsymmetrical Tridentate Binding Units by a Protonated Covalent Tripod
• Authors of publication: Fabien Renaud; Claude Piguet; Gérald Bernardinelli; Jean-Claude Bünzli; Gérard Hopfgartner
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 9326 - 9342
• a: 13.2949 ± 0.0005 Å
• b: 13.2949 ± 0.0005 Å
• c: 61.02 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 9340.6 ± 0.7 ų
• Cell temperature: 200 K
• Number of distinct elements: 8
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.062
• Goodness-of-fit parameter for all reflections included in the refinement: 2.687
• Diffraction radiation wavelength: 1.54183 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No