Information card for entry 4116563

Structure parameters

• Formula: C30 H60 Ga K N2 O8
• Calculated formula: C30 H60 Ga K N2 O8
• Title of publication: A Carbene Analogue with Low-Valent Gallium as a Heteroatom in a quasi-Aromatic Imidazolate Anion
• Authors of publication: Eva S. Schmidt; Alexander Jockisch; Hubert Schmidbaur
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 9758 - 9759
• a: 9.718 ± 0.002 Å
• b: 10.116 ± 0.002 Å
• c: 10.318 ± 0.002 Å
• α: 77.67 ± 0.02°
• β: 69.64 ± 0.02°
• γ: 88.51 ± 0.02°
• Cell volume: 927.7 ± 0.4 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0857
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No