Information card for entry 4116737

Structure parameters

• Formula: C48 H48 Cl2 Li2 N8 Nb2 O2
• Calculated formula: C46 H20 Cl2 Li2 N8 Nb2 O4
• Title of publication: Triply Bonded Nb24+ Tetragonal Lantern Compounds: Some Accompanied by Novel B-H...Na+ Interactions
• Authors of publication: F. Albert Cotton; John H. Matonic; Carlos A. Murillo
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1998
• Journal volume: 120
• Pages of publication: 6047 - 6052
• a: 14.1 ± 0.002 Å
• b: 14.1 ± 0.002 Å
• c: 11.614 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2309 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0611
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for all reflections: 0.1386
• Weighted residual factors for significantly intense reflections: 0.1272
• Goodness-of-fit parameter for all reflections: 1.147
• Goodness-of-fit parameter for significantly intense reflections: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No