Information card for entry 4116957

Structure parameters

• Formula: C36 H59 B Fe P4
• Calculated formula: C36 H59 B Fe P4
• Title of publication: Synthesis, Structural Diversity, Dynamics, and Acidity of the M(II) and M(IV) Complexes [MH3(PR3)4]+ (M = Fe, Ru, Os; R = Me, Et)
• Authors of publication: Dmitry G. Gusev; Rainer Hübener; Peter Burger; Olli Orama; Heinz Berke
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1997
• Journal volume: 119
• Pages of publication: 3716 - 3731
• a: 15.899 ± 0.003 Å
• b: 12.702 ± 0.002 Å
• c: 20.169 ± 0.004 Å
• α: 90°
• β: 110.39 ± 0.02°
• γ: 90°
• Cell volume: 3817.9 ± 1.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 6.15
• Residual factor for significantly intense reflections: 4.87
• Weighted residual factors for all reflections: 16.32
• Weighted residual factors for significantly intense reflections: 5.48
• Goodness-of-fit parameter for significantly intense reflections: 1.97
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No