Information card for entry 4117398

Structure parameters

• Formula: C27 H31 Cl N2 O5 Si W
• Calculated formula: C27 H31 Cl N2 O5 Si W
• SMILES: C(#[O])[W](C#[O])(C#[O])(C#[O])(C#[O])[Si]1([N](C(C)(C)C)=C(c2ccccc2)N1C(C)(C)C)Cl.c1cc(ccc1)C
• Title of publication: Stabilization of Low Valent Silicon Fluorides in the Coordination Sphere of Transition Metals
• Authors of publication: Ramachandran Azhakar; Rajendra S. Ghadwal; Herbert W. Roesky; Hilke Wolf; Dietmar Stalke
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 2423 - 2428
• a: 9.873 ± 0.002 Å
• b: 11.621 ± 0.003 Å
• c: 13.126 ± 0.001 Å
• α: 94.91 ± 0.01°
• β: 93.04 ± 0.02°
• γ: 97.56 ± 0.01°
• Cell volume: 1484.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0211
• Residual factor for significantly intense reflections: 0.0205
• Weighted residual factors for significantly intense reflections: 0.0509
• Weighted residual factors for all reflections included in the refinement: 0.0514
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.5608 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No