Information card for entry 4117938

Structure parameters

• Formula: C28 H39 N O
• Calculated formula: C28 H38.66 N O
• Title of publication: Total Syntheses of Anominine and Tubingensin A
• Authors of publication: Ming Bian; Zhen Wang; Xiaochun Xiong; Yu Sun; Carlo Matera; K. C. Nicolaou; Ang Li
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 8078 - 8081
• a: 9.3676 ± 0.0008 Å
• b: 10.5455 ± 0.0009 Å
• c: 13.8622 ± 0.0011 Å
• α: 88.235 ± 0.002°
• β: 72.615 ± 0.002°
• γ: 63.819 ± 0.002°
• Cell volume: 1164.57 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0566
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1314
• Weighted residual factors for all reflections included in the refinement: 0.1401
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No