Information card for entry 4118063

Structure parameters

• Common name: apx1346
• Formula: C54 H63 Br Cl I3 N6 U
• Calculated formula: C54 H63 Br Cl I3 N6 U
• Title of publication: A Direct Route to Bis(imido)uranium(V) Halides via Metathesis of Uranium Tetrachloride
• Authors of publication: Robert E. Jilek; Liam P. Spencer; Richard A. Lewis; Brian L. Scott; Trevor W. Hayton; James M. Boncella
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 9876 - 9878
• a: 14.5626 ± 0.0011 Å
• b: 23.1936 ± 0.0018 Å
• c: 36.78 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12422.8 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.111
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for significantly intense reflections: 0.1623
• Weighted residual factors for all reflections included in the refinement: 0.1744
• Goodness-of-fit parameter for all reflections included in the refinement: 1.383
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No