Information card for entry 4118105

Structure parameters

• Chemical name: bis(bipyridine) nitrosyl nickel hexafluorophosphate
• Formula: C22 H20 Cl3 F6 N5 Ni O P
• Calculated formula: C22 H20 Cl3 F6 N5 Ni O P
• Title of publication: Formation of N2O from a Nickel Nitrosyl: Isolation of the cis-[N2O2]2- Intermediate
• Authors of publication: Ashley M. Wright; Guang Wu; Trevor W. Hayton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 9930 - 9933
• a: 9.1746 ± 0.0012 Å
• b: 12.0587 ± 0.0016 Å
• c: 12.7075 ± 0.0016 Å
• α: 91.115 ± 0.002°
• β: 102.721 ± 0.002°
• γ: 107.306 ± 0.002°
• Cell volume: 1303.8 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0602
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for significantly intense reflections: 0.1249
• Weighted residual factors for all reflections included in the refinement: 0.1322
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No