Information card for entry 4118343

Structure parameters

• Formula: C184 H140 Cl8 N12 O24 Pd12
• Calculated formula: C184 H140 Cl8 N12 O24 Pd12
• Title of publication: Connecting Binuclear Pd(III) and Mononuclear Pd(IV) Chemistry by Pd-Pd Bond Cleavage
• Authors of publication: David C. Powers; Eunsung Lee; Alireza Ariafard; Melanie S. Sanford; Brian F. Yates; Allan J. Canty; Tobias Ritter
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 12002 - 12009
• a: 17.1241 ± 0.0006 Å
• b: 20.2806 ± 0.0007 Å
• c: 23.2979 ± 0.0009 Å
• α: 89.559 ± 0.002°
• β: 89.23 ± 0.002°
• γ: 88.773 ± 0.002°
• Cell volume: 8088.3 ± 0.5 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.0956
• Weighted residual factors for all reflections included in the refinement: 0.1069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No