Information card for entry 4118413

Structure parameters

• Formula: C124 H162 N2 O8 U2
• Calculated formula: C124 H152 N2 O8 U2
• Title of publication: Uranium(III)-Mediated C-C-Coupling of Terminal Alkynes: Formation of Dinuclear Uranium(IV) Vinyl Complexes
• Authors of publication: Boris Kosog; Christos E. Kefalidis; Frank W. Heinemann; Laurent Maron; Karsten Meyer
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 12792 - 12797
• a: 15.308 ± 0.002 Å
• b: 16.227 ± 0.0008 Å
• c: 22.224 ± 0.003 Å
• α: 102.031 ± 0.005°
• β: 101.942 ± 0.009°
• γ: 91.137 ± 0.008°
• Cell volume: 5270.9 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections included in the refinement: 0.0802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No