Information card for entry 4118573

Structure parameters

• Formula: C69.5 H92 Ge2
• Calculated formula: C69.5 H92 Ge2
• Title of publication: The Role of Group 14 Element Hydrides in the Activation of C-H Bonds in Cyclic Olefins
• Authors of publication: Owen T. Summerscales; Christine A. Caputo; Caroline E. Knapp; James C. Fettinger; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 14595 - 14603
• a: 20.5795 ± 0.0016 Å
• b: 13.4167 ± 0.001 Å
• c: 22.7242 ± 0.0017 Å
• α: 90°
• β: 109.826 ± 0.002°
• γ: 90°
• Cell volume: 5902.5 ± 0.8 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0283
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0737
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No