Information card for entry 4118659

Structure parameters

• Formula: C42 H59 N3 O Pd
• Calculated formula: C42.002 H59.007 N3 O Pd
• Title of publication: Reductive Elimination of Alkylamines from Low-Valent, Alkylpalladium(II) Amido Complexes
• Authors of publication: Patrick S. Hanley; Seth L. Marquard; Thomas R. Cundari; John F. Hartwig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 15281 - 15284
• a: 12.8298 ± 0.0003 Å
• b: 15.947 ± 0.0003 Å
• c: 19.8577 ± 0.0004 Å
• α: 90°
• β: 108.184 ± 0.001°
• γ: 90°
• Cell volume: 3859.92 ± 0.14 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0437
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.1023
• Weighted residual factors for all reflections included in the refinement: 0.1056
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No