Information card for entry 4118813

Structure parameters

• Chemical name: bis(trimethylsilyl)diazomethane
• Formula: C7 H18 N2 Si2
• Calculated formula: C7 H18 N2 Si2
• SMILES: [Si](C([Si](C)(C)C)=N#N)(C)(C)C
• Title of publication: Catalytic Trimerization of Bis-silylated Diazomethane
• Authors of publication: Muhammad Farooq Ibad; Peter Langer; Fabian Reiß; Axel Schulz; Alexander Villinger
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 17757 - 17768
• a: 9.3503 ± 0.0003 Å
• b: 12.6572 ± 0.0004 Å
• c: 12.7666 ± 0.0004 Å
• α: 117.845 ± 0.001°
• β: 110.488 ± 0.001°
• γ: 91.987 ± 0.001°
• Cell volume: 1215.12 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0493
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.1035
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No