Crystallography Open Database

Information card for entry 4118817

Preview

Structure parameters

Chemical name	N,N-bis(trimethylsilyl)amino-N-(trimethylsilyl)nitrilium tetrakis(pentafluorophenyl)borate
Formula	C34 H27 B F20 N2 Si3
Calculated formula	C34 H27 B F20 N2 Si3
Title of publication	Catalytic Trimerization of Bis-silylated Diazomethane
Authors of publication	Muhammad Farooq Ibad; Peter Langer; Fabian Reiß; Axel Schulz; Alexander Villinger
Journal of publication	Journal of the American Chemical Society
Year of publication	2012
Journal volume	134
Pages of publication	17757 - 17768
a	16.8136 ± 0.0004 Å
b	12.8837 ± 0.0003 Å
c	19.1298 ± 0.0005 Å
α	90°
β	104.172 ± 0.001°
γ	90°
Cell volume	4017.8 ± 0.17 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0654
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.0992
Weighted residual factors for all reflections included in the refinement	0.1078
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4118817.html