Crystallography Open Database

Information card for entry 4118839

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Structure parameters

Formula	C24 H52 Co N2 O4
Calculated formula	C24 H52 Co N2 O4
SMILES	C(=O)(CCCCCCCCCCC)O[Co]([NH3])([NH3])OC(=O)CCCCCCCCCCC
Title of publication	The Big Impact of a Small Detail: Cobalt Nanocrystal Polymorphism as a Result of Precursor Addition Rate during Stock Solution Preparation
Authors of publication	Nikos Liakakos; Benoît Cormary; Xiaojian Li; Pierre Lecante; Marc Respaud; Laurent Maron; Andrea Falqui; Alessandro Genovese; Laure Vendier; Spyros Koïnis; Bruno Chaudret; Katerina Soulantica
Journal of publication	Journal of the American Chemical Society
Year of publication	2012
Journal volume	134
Pages of publication	17922 - 17931
a	51.02 ± 0.01 Å
b	5.7091 ± 0.0011 Å
c	9.941 ± 0.002 Å
α	90°
β	94.55 ± 0.03°
γ	90°
Cell volume	2886.5 ± 1 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0968
Residual factor for significantly intense reflections	0.0636
Weighted residual factors for significantly intense reflections	0.1208
Weighted residual factors for all reflections included in the refinement	0.1356
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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