Crystallography Open Database

Information card for entry 4120993

4120992 << 4120993 >> 4120994

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Structure parameters

Formula	C208 H198 Cl18 O112 U38
Calculated formula	C208 H200 Cl18 O114 U38
Title of publication	Isolation of the Large {Actinide}38 Poly-oxo Cluster with Uranium
Authors of publication	Clément Falaise; Christophe Volkringer; Jean-François Vigier; Arnaud Beaurain; Pascal Roussel; Pierre Rabu; Thierry Loiseau
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	15678 - 15681
a	21.9986 ± 0.0003 Å
b	21.9986 ± 0.0003 Å
c	29.9603 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	14498.9 ± 0.4 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0799
Residual factor for significantly intense reflections	0.0477
Weighted residual factors for significantly intense reflections	0.0631
Weighted residual factors for all reflections included in the refinement	0.0647
Goodness-of-fit parameter for significantly intense reflections	2.32
Goodness-of-fit parameter for all reflections included in the refinement	1.94
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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