Crystallography Open Database

Information card for entry 4121215

Preview

Coordinates	4121215.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C126 H154 N4 P6 Pt4 Si6
Calculated formula	C126 H154 N4 P6 Pt4 Si6
Title of publication	From a Zwitterionic Phosphasilene to Base Stabilized Silyliumylidene-Phosphide and Bis(silylene) Complexes
Authors of publication	Nora C. Breit; Tibor Szilvási; Tsuyoshi Suzuki; Daniel Gallego; Shigeyoshi Inoue
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	17958 - 17968
a	10.068 ± 0.005 Å
b	24.162 ± 0.005 Å
c	26.174 ± 0.005 Å
α	90 ± 0.005°
β	99.656 ± 0.005°
γ	90 ± 0.005°
Cell volume	6277 ± 4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0437
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.0957
Weighted residual factors for all reflections included in the refinement	0.0978
Goodness-of-fit parameter for all reflections included in the refinement	1.447
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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