Information card for entry 4121217

Structure parameters

• Common name: TPPN (1)
• Chemical name: 1,8-Bis(trispyrrolidinophosphazenyl)naphthalene
• Formula: C36 H57 N9 P2
• Calculated formula: C36 H57 N9 P2
• Title of publication: A New Synthetic Pathway to the Second and Third Generation of Superbasic Bisphosphazene Proton Sponges: The Run for the Best Chelating Ligand for a Proton
• Authors of publication: Julius F. Kögel; Benjamin Oelkers; Borislav Kovačević; Jörg Sundermeyer
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 17768 - 17774
• a: 16.2714 ± 0.0017 Å
• b: 13.8754 ± 0.0012 Å
• c: 16.5807 ± 0.0015 Å
• α: 90°
• β: 104.427 ± 0.003°
• γ: 90°
• Cell volume: 3625.4 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0821
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1091
• Weighted residual factors for all reflections included in the refinement: 0.1276
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No