Information card for entry 4121288

Structure parameters

• Formula: C37 H58 Br N2 Ni Si2
• Calculated formula: C37 H58 Br N2 Ni Si2
• Title of publication: Synthesis and Reactivity of Two-Coordinate Ni(I) Alkyl and Aryl Complexes
• Authors of publication: Carl A. Laskowski; Donald J. Bungum; Steven M. Baldwin; Sarah A. Del Ciello; Vlad M. Iluc; Gregory L. Hillhouse
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 18272 - 18275
• a: 12.369 ± 0.003 Å
• b: 16.924 ± 0.003 Å
• c: 18.452 ± 0.004 Å
• α: 90°
• β: 108.08 ± 0.03°
• γ: 90°
• Cell volume: 3671.9 ± 1.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1833
• Residual factor for significantly intense reflections: 0.1001
• Weighted residual factors for significantly intense reflections: 0.1731
• Weighted residual factors for all reflections included in the refinement: 0.2028
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No