Information card for entry 4122382

Structure parameters

• Formula: C30 H34 N2 O2
• Calculated formula: C30 H34 N2 O2
• SMILES: O=C(N1CCCC2=C1C[C@H]1C[C@H](C[C@]32N(CCC[C@@H]13)C(=O)c1ccccc1)C)c1ccccc1
• Title of publication: Biogenetically inspired total syntheses of lycopodium alkaloids, (+)-flabellidine and (-)-lycodine.
• Authors of publication: Azuma, Masayuki; Yoshikawa, Tetsuya; Kogure, Noriyuki; Kitajima, Mariko; Takayama, Hiromitsu
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 33
• Pages of publication: 11618 - 11621
• a: 10.9517 ± 0.0002 Å
• b: 9.02967 ± 0.00016 Å
• c: 13.0861 ± 0.0003 Å
• α: 90°
• β: 105.544 ± 0.001°
• γ: 90°
• Cell volume: 1246.76 ± 0.04 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for all reflections included in the refinement: 0.1137
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No