Information card for entry 4123225

Structure parameters

• Common name: 5
• Formula: C31 H54 N4 Si4 Y
• Calculated formula: C31 H54 N4 Si4 Y
• SMILES: [Y](N([Si](C)(C)C)[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)(N(Cc1ccccc1)Cc1ccccc1)[n]1ccccc1
• Title of publication: Aminomethylation Reaction of ortho-Pyridyl C-H Bonds Catalyzed by Group 3 Metal Triamido Complexes.
• Authors of publication: Nagae, Haruki; Shibata, Yu; Tsurugi, Hayato; Mashima, Kazushi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 2
• Pages of publication: 640 - 643
• a: 30.617 ± 0.008 Å
• b: 17.608 ± 0.005 Å
• c: 21.674 ± 0.006 Å
• α: 90°
• β: 100.565 ± 0.003°
• γ: 90°
• Cell volume: 11486 ± 5 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1331
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1451
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No