Information card for entry 4123238
| Formula |
C65 H68 B F24 P2 Rh |
| Calculated formula |
C65 H68 B F24 P2 Rh |
| Title of publication |
Solid-State Synthesis and Characterization of σ-Alkane Complexes, [Rh(L2)(η(2),η(2)-C7H12)][BAr(F)4] (L2 = Bidentate Chelating Phosphine). |
| Authors of publication |
Pike, Sebastian D.; Chadwick, F. Mark; Rees, Nicholas H.; Scott, Mark P.; Weller, Andrew S.; Krämer, Tobias; Macgregor, Stuart A. |
| Journal of publication |
Journal of the American Chemical Society |
| Year of publication |
2015 |
| Journal volume |
137 |
| Journal issue |
2 |
| Pages of publication |
820 - 833 |
| a |
12.8259 ± 0.0003 Å |
| b |
13.0175 ± 0.0003 Å |
| c |
19.8317 ± 0.0004 Å |
| α |
93.0486 ± 0.0019° |
| β |
90.1923 ± 0.0018° |
| γ |
96.187 ± 0.002° |
| Cell volume |
3287.04 ± 0.13 Å3 |
| Cell temperature |
150 K |
| Ambient diffraction temperature |
150 K |
| Ambient diffracton pressure |
101 kPa |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0815 |
| Residual factor for significantly intense reflections |
0.0792 |
| Weighted residual factors for all reflections |
0.2403 |
| Weighted residual factors for significantly intense reflections |
0.2399 |
| Weighted residual factors for all reflections included in the refinement |
0.2403 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.0761 |
| Diffraction radiation wavelength |
1.5418 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4123238.html
