Total Syntheses of (-)-Mersicarpine, (-)-Scholarisine G, (+)-Melodinine E, (-)-Leuconoxine, (-)-Leuconolam, (-)-Leuconodine A, (+)-Leuconodine F, and (-)-Leuconodine C: Self-Induced Diastereomeric Anisochronism (SIDA) Phenomenon for Scholarisine G and Leuconodines A and C.
Authors of publication
Xu, Zhengren; Wang, Qian; Zhu, Jieping
Journal of publication
Journal of the American Chemical Society
Year of publication
2015
Journal volume
137
Journal issue
20
Pages of publication
6712 - 6724
a
17.3461 ± 0.0002 Å
b
13.787 ± 0.0002 Å
c
7.60339 ± 0.00011 Å
α
90°
β
90°
γ
90°
Cell volume
1818.36 ± 0.04 Å3
Cell temperature
140 ± 2 K
Ambient diffraction temperature
140 ± 2 K
Number of distinct elements
4
Space group number
18
Hermann-Mauguin space group symbol
P 21 21 2
Hall space group symbol
P 2 2ab
Residual factor for all reflections
0.0355
Residual factor for significantly intense reflections
0.0347
Weighted residual factors for significantly intense reflections
0.0963
Weighted residual factors for all reflections included in the refinement
0.0977
Goodness-of-fit parameter for all reflections included in the refinement
