Information card for entry 4125735

Structure parameters

• Formula: C51 H52 F6 N2 O4 P Sb
• Calculated formula: C51 H52 F6 N2 O4 P Sb
• Title of publication: Enantioselective Synthesis of [6]Carbohelicenes.
• Authors of publication: González-Fernández, Elisa; Nicholls, Leo D. M.; Schaaf, Lukas D.; Farès, Christophe; Lehmann, Christian W.; Alcarazo, Manuel
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 4
• Pages of publication: 1428 - 1431
• a: 11.7711 ± 0.0017 Å
• b: 18.123 ± 0.003 Å
• c: 12.1515 ± 0.0018 Å
• α: 90°
• β: 113.687 ± 0.003°
• γ: 90°
• Cell volume: 2373.9 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No