Information card for entry 4126227

Structure parameters

• Formula: C26 H47 B O Si
• Calculated formula: C26 H47 B O Si
• Title of publication: Uncatalyzed Carboboration of Seven-Membered-Ring trans-Alkenes: Formation of Air-Stable Trialkylboranes.
• Authors of publication: Sanzone, Jillian R.; Hu, Chunhua T.; Woerpel, K. A.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 25
• Pages of publication: 8404 - 8407
• a: 10.3814 ± 0.0004 Å
• b: 8.5313 ± 0.0003 Å
• c: 30.7969 ± 0.0011 Å
• α: 90°
• β: 99.6603 ± 0.0005°
• γ: 90°
• Cell volume: 2688.91 ± 0.17 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No