Crystallography Open Database

Information card for entry 4128279

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Coordinates	4128279.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H108 O16 Si4 Tb
Calculated formula	C48 H108 O16 Si4 Tb
Title of publication	Molecular Complex of Tb in the +4 Oxidation State.
Authors of publication	Palumbo, Chad T.; Zivkovic, Ivica; Scopelliti, Rosario; Mazzanti, Marinella
Journal of publication	Journal of the American Chemical Society
Year of publication	2019
Journal volume	141
Journal issue	25
Pages of publication	9827 - 9831
a	24.0696 ± 0.0005 Å
b	13.4628 ± 0.0002 Å
c	40.7459 ± 0.0008 Å
α	90°
β	96.4478 ± 0.0017°
γ	90°
Cell volume	13120 ± 0.4 Å³
Cell temperature	140 ± 0.1 K
Ambient diffraction temperature	140 ± 0.1 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0595
Residual factor for significantly intense reflections	0.0518
Weighted residual factors for significantly intense reflections	0.1218
Weighted residual factors for all reflections included in the refinement	0.1266
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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