Information card for entry 4128432

Structure parameters

• Formula: C25 H29 Cr O4.58
• Calculated formula: C25 H29 Cr O4.583
• Title of publication: Robust Chromium Precursors for Catalysis: Isolation and Structure of a Single-Component Ethylene Tetramerization Precatalyst.
• Authors of publication: Hirscher, Nathanael A.; Perez Sierra, Danny; Agapie, Theodor
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 14
• Pages of publication: 6022 - 6029
• a: 20.0935 ± 0.001 Å
• b: 11.1921 ± 0.0006 Å
• c: 10.9889 ± 0.0005 Å
• α: 90°
• β: 116.859 ± 0.002°
• γ: 90°
• Cell volume: 2204.68 ± 0.19 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.05 K
• Number of distinct elements: 4
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No