Information card for entry 4128660

Structure parameters

• Formula: C16 H36 Cl3 N S Si
• Calculated formula: C16 H36 Cl3 N S Si
• Title of publication: Orthophosphate and Sulfate Utilization for C-E (E = P, S) Bond Formation via Trichlorosilyl Phosphide and Sulfide Anions.
• Authors of publication: Geeson, Michael B.; Ríos, Pablo; Transue, Wesley J.; Cummins, Christopher C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 15
• Pages of publication: 6375 - 6384
• a: 17.253 ± 0.012 Å
• b: 15.242 ± 0.011 Å
• c: 18.394 ± 0.013 Å
• α: 90°
• β: 103.363 ± 0.012°
• γ: 90°
• Cell volume: 4706 ± 6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0778
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1436
• Weighted residual factors for all reflections included in the refinement: 0.158
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No