Information card for entry 4128663

Structure parameters

• Formula: C48 H32 B4 F22
• Calculated formula: C48 H32 B4 F22
• Title of publication: Activation of H₂ and Et₃SiH by the Borinium Cation [Mes₂B]⁺: Avenues to Cations [MesB(μ-H)₂(μ-Mes)BMes]⁺ and [H₂B(μ-H)(μ-Mes)B(μ-Mes)(μ-H)BH₂]<sup/>.
• Authors of publication: Bamford, Karlee L.; Qu, Zheng-Wang; Stephan, Douglas W.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 15
• Pages of publication: 6180 - 6184
• a: 16.7541 ± 0.0018 Å
• b: 20.7321 ± 0.0017 Å
• c: 26.318 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9141.5 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0938
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.1479
• Weighted residual factors for all reflections included in the refinement: 0.1862
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No