Iodonitrene in Action: Direct Transformation of Amino Acids into Terminal Diazirines and <sup>15</sup>N<sub>2</sub>-Diazirines and Their Application as Hyperpolarized Markers.
Authors of publication
Glachet, Thomas; Marzag, Hamid; Saraiva Rosa, Nathalie; Colell, Johannes F. P.; Zhang, Guannan; Warren, Warren S.; Franck, Xavier; Theis, Thomas; Reboul, Vincent
Journal of publication
Journal of the American Chemical Society
Year of publication
2019
Journal volume
141
Journal issue
34
Pages of publication
13689 - 13696
a
10.1878 ± 0.0016 Å
b
7.9625 ± 0.0015 Å
c
19.59 ± 0.003 Å
α
90°
β
99.557 ± 0.007°
γ
90°
Cell volume
1567.1 ± 0.5 Å3
Cell temperature
149 ± 2 K
Ambient diffraction temperature
149 ± 2 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.1439
Residual factor for significantly intense reflections
0.0778
Weighted residual factors for significantly intense reflections
0.1634
Weighted residual factors for all reflections included in the refinement
0.1944
Goodness-of-fit parameter for all reflections included in the refinement
