Information card for entry 4129578

Structure parameters

• Formula: C56 H53 B F4 N O2 P2 Rh
• Calculated formula: C56 H53 B F4 N O2 P2 Rh
• Title of publication: Anti-Markovnikov Hydroamination of Homoallylic Amines.
• Authors of publication: Ensign, Seth C.; Vanable, Evan P.; Kortman, Gregory D.; Weir, Lee J.; Hull, Kami L.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 43
• Pages of publication: 13748 - 13751
• a: 10.5541 ± 0.0006 Å
• b: 10.8702 ± 0.0006 Å
• c: 21.4812 ± 0.001 Å
• α: 88.2639 ± 0.0019°
• β: 84.3786 ± 0.0018°
• γ: 73.4287 ± 0.0019°
• Cell volume: 2350.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0261
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0599
• Weighted residual factors for all reflections included in the refinement: 0.061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No