Information card for entry 4130159

Structure parameters

• Formula: C155 H164 Cl4 O12 P4 Pd2
• Calculated formula: C155 H164 Cl4 O12 P4 Pd2
• Title of publication: Enantioselective Aminomethylamination of Conjugated Dienes with Aminals Enabled by Chiral Palladium Complex-Catalyzed C-N Bond Activation.
• Authors of publication: Liu, Yang; Xie, Yinjun; Wang, Hongli; Huang, Hanmin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 13
• Pages of publication: 4314 - 4317
• a: 15.041 ± 0.002 Å
• b: 20.148 ± 0.003 Å
• c: 24.408 ± 0.004 Å
• α: 90°
• β: 93.946 ± 0.003°
• γ: 90°
• Cell volume: 7379.2 ± 1.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0811
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1505
• Weighted residual factors for all reflections included in the refinement: 0.1651
• Goodness-of-fit parameter for all reflections included in the refinement: 0.991
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No