Information card for entry 4130764

Structure parameters

• Formula: C119 H195 Cu Ge18 N P3 Pd3 Sn7
• Calculated formula: C119 H195 Cu Ge18 N P3 Pd3 Sn7
• Title of publication: A Stannyl-Decorated Zintl Ion [Ge18Pd3(Sn(i)Pr3)6](2-): Twinned Icosahedron with a Common Pd3-Face or 18-Vertex Hypho-Deltahedron with a Pd3-Triangle Inside.
• Authors of publication: Perla, Luis G.; Sevov, Slavi C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 31
• Pages of publication: 9795 - 9798
• a: 14.669 ± 0.0011 Å
• b: 22.4404 ± 0.0018 Å
• c: 23.8287 ± 0.0019 Å
• α: 79.329 ± 0.003°
• β: 75.196 ± 0.002°
• γ: 80.078 ± 0.003°
• Cell volume: 7387.6 ± 1 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1027
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No