Information card for entry 4130785

Structure parameters

• Formula: C313 H183 F48 Fe4 N26 Sb8
• Calculated formula: C313 H183 F23.1 Fe4 N26 Sb3.85
• Title of publication: Pathway-Dependent Post-assembly Modification of an Anthracene-Edged M(II)4L6 Tetrahedron.
• Authors of publication: Ronson, Tanya K.; Pilgrim, Ben S.; Nitschke, Jonathan R.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 33
• Pages of publication: 10417 - 10420
• a: 21.8874 ± 0.0008 Å
• b: 27.4261 ± 0.0009 Å
• c: 30.8088 ± 0.0009 Å
• α: 64.666 ± 0.002°
• β: 87.269 ± 0.002°
• γ: 79.937 ± 0.002°
• Cell volume: 16450.7 ± 1 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1308
• Residual factor for significantly intense reflections: 0.109
• Weighted residual factors for significantly intense reflections: 0.3123
• Weighted residual factors for all reflections included in the refinement: 0.3387
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No