Information card for entry 4132737

Structure parameters

• Formula: C17 H36 Cl9 N Si3
• Calculated formula: C16.9998 H35.9991 Cl9 N Si3
• Title of publication: Exhaustively Trichlorosilylated C₁ and C₂ Building Blocks: Beyond the Müller-Rochow Direct Process.
• Authors of publication: Georg, Isabelle; Teichmann, Julian; Bursch, Markus; Tillmann, Jan; Endeward, Burkhard; Bolte, Michael; Lerner, Hans-Wolfram; Grimme, Stefan; Wagner, Matthias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 30
• Pages of publication: 9696 - 9708
• a: 18.5044 ± 0.0008 Å
• b: 18.5044 ± 0.0008 Å
• c: 18.5044 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6336.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 218
• Hermann-Mauguin space group symbol: P -4 3 n
• Hall space group symbol: P -4n 2 3
• Residual factor for all reflections: 0.0517
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0844
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No