Information card for entry 4133398

Structure parameters

• Formula: C54 H56 Cl4 Ge2 N2 O4 Zn
• Calculated formula: C54 H56 Cl4 Ge2 N2 O4 Zn
• Title of publication: Radical Germylzincation of α-Heteroatom-Substituted Alkynes.
• Authors of publication: de la Vega-Hernández, Karen; Romain, Elise; Coffinet, Anais; Bijouard, Kajetan; Gontard, Geoffrey; Chemla, Fabrice; Ferreira, Franck; Jackowski, Olivier; Perez-Luna, Alejandro
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17632 - 17642
• a: 13.4291 ± 0.0006 Å
• b: 17.2102 ± 0.0008 Å
• c: 23.7226 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5482.7 ± 0.4 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1609
• Weighted residual factors for all reflections included in the refinement: 0.1732
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No