Information card for entry 4133534

Structure parameters

• Formula: C450 H540 N45 O323.5 S12 V65 W15
• Calculated formula: C350 O264 V60 W12
• Title of publication: Self-Assembly of Goldberg Polyhedra from a Concave [WV₅O₁₁(RCO₂)₅(SO₄)]^3- Building Block with 5-Fold Symmetry.
• Authors of publication: Zhang, Yuteng; Gan, Hongmei; Qin, Chao; Wang, Xinlong; Su, Zhongmin; Zaworotko, Michael J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17365 - 17368
• a: 43.2511 ± 0.0016 Å
• b: 43.2511 ± 0.0016 Å
• c: 39.0469 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 73043 ± 5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.02 K
• Number of distinct elements: 7
• Space group number: 131
• Hermann-Mauguin space group symbol: P 42/m m c
• Hall space group symbol: -P 4c 2
• Residual factor for all reflections: 0.13
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for significantly intense reflections: 0.2223
• Weighted residual factors for all reflections included in the refinement: 0.2612
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No