Information card for entry 4133536

Structure parameters

• Formula: C556 H544 N98 O304 S12 V60 W12
• Calculated formula: C480 H240 N60 O304 S12 V60 W12
• Title of publication: Self-Assembly of Goldberg Polyhedra from a Concave [WV₅O₁₁(RCO₂)₅(SO₄)]^3- Building Block with 5-Fold Symmetry.
• Authors of publication: Zhang, Yuteng; Gan, Hongmei; Qin, Chao; Wang, Xinlong; Su, Zhongmin; Zaworotko, Michael J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17365 - 17368
• a: 41.174 ± 0.005 Å
• b: 41.174 ± 0.005 Å
• c: 53.404 ± 0.014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 90536 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 131
• Hermann-Mauguin space group symbol: P 42/m m c
• Hall space group symbol: -P 4c 2
• Residual factor for all reflections: 0.3943
• Residual factor for significantly intense reflections: 0.2105
• Weighted residual factors for significantly intense reflections: 0.4703
• Weighted residual factors for all reflections included in the refinement: 0.535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.41
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No