Information card for entry 4135393

Structure parameters

• Formula: C131 H141 Cl4 F3 N12 P8 Pd4
• Calculated formula: C131 H141 Cl4 F3 N12 P8 Pd4
• Title of publication: Enthalpy-Controlled Insertion of a "Nonspectator" Tricoordinate Phosphorus Ligand into Group 10 Transition Metal-Carbon Bonds.
• Authors of publication: Hwang, Seung Jun; Tanushi, Akira; Radosevich, Alexander T.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 51
• Pages of publication: 21285 - 21291
• a: 15.426 ± 0.003 Å
• b: 15.426 ± 0.003 Å
• c: 26.835 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6386 ± 2 ų
• Cell temperature: 15 ± 2 K
• Ambient diffraction temperature: 15 K
• Number of distinct elements: 7
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.1018
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.24797 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No