Information card for entry 4300025

Structure parameters

• Formula: C99.37 H10.74 Bi8 Cl6.74 F80 O22
• Calculated formula: C99.38 H10.76 Bi8 Cl6.76 F80 O22
• Title of publication: Oligomerization and Oxide Formation in Bismuth Aryl Alkoxides: Synthesis and Characterization of Bi4(μ4-O)(μ-OC6F5)6{μ3-OBi(μ-OC6F5)3}2(C6H5CH3), Bi8(μ4-O)2(μ3-O)2(μ-OC6F5)16, Bi6(μ3-O)4(μ3-OC6F5){μ3-OBi(OC6F5)4}3, NaBi4(μ3-O)2(OC6F5)9(THF)2, and Na2Bi4(μ3-O)2(OC6F5)10(THF)2
• Authors of publication: Kenton H. Whitmire; Silke Hoppe; Orson Sydora; Jennifer L. Jolas; Carolyn M. Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 85 - 97
• a: 14.292 ± 0.003 Å
• b: 15.111 ± 0.003 Å
• c: 17.545 ± 0.004 Å
• α: 112.19 ± 0.03°
• β: 104.46 ± 0.03°
• γ: 100.58 ± 0.03°
• Cell volume: 3230 ± 1.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for all reflections: 0.1015
• Weighted residual factors for significantly intense reflections: 0.0931
• Goodness-of-fit parameter for all reflections: 1.048
• Goodness-of-fit parameter for significantly intense reflections: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No