Polynuclear Magnesium and Magnesium-Titanium Species. Syntheses and Crystal Structures of [Mg4(μ3,η2-ddbfo)2(μ,η2-ddbfo)2(μ,η1-ddbfo)2(η1-ddbfo)2], [Mg4(μ3-OMe)2(μ,η2-ddbfo)2(μ,η1-ddbfo)2(η1-ddbfo)2(CH3OH)5], and [Mg4(μ3,η2-thffo)2(μ,η2-thffo)2(μ,η1-thffo)2{μ-OTi(DIPP)3}2] Aggregates
Authors of publication
Piotr Sobota; Józef Utko; Katarzyna Sztajnowska; Jolanta Ejfler; Lucjan B. Jerzykiewicz
Journal of publication
Inorganic Chemistry
Year of publication
2000
Journal volume
39
Pages of publication
235 - 239
a
12.053 ± 0.002 Å
b
12.09 ± 0.002 Å
c
26.864 ± 0.005 Å
α
90°
β
98.5 ± 0.03°
γ
90°
Cell volume
3871.6 ± 1.2 Å3
Cell temperature
100 ± 0.4 K
Ambient diffraction temperature
100 ± 0.4 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0504
Residual factor for significantly intense reflections
0.0482
Weighted residual factors for significantly intense reflections
0.111
Weighted residual factors for all reflections included in the refinement
0.1132
Goodness-of-fit parameter for all reflections included in the refinement
