Information card for entry 4300134

Structure parameters

• Common name: 1, Au2Na(dppn)3(PF6)3 4.5CH3CN 0.5 Et2O
• Formula: C107 H72 Au2 F18 N10.5 Na O0.5 P9
• Calculated formula: C107 H72 Au2 F18 N10.5 Na O0.5 P9
• Title of publication: Gold(I) and Silver(I) Metallocryptates Based on 2,9-Bis(diphenylphosphino)-1,8-naphthyridine
• Authors of publication: Vincent J. Catalano; Heidi M. Kar; Byron L. Bennett
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 121 - 127
• a: 15.408 ± 0.003 Å
• b: 17.295 ± 0.003 Å
• c: 22.425 ± 0.005 Å
• α: 73.68 ± 0.01°
• β: 77.32 ± 0.01°
• γ: 74.18 ± 0.01°
• Cell volume: 5451.4 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.105
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for all reflections: 0.1359
• Weighted residual factors for significantly intense reflections: 0.1128
• Goodness-of-fit parameter for all reflections: 1.063
• Goodness-of-fit parameter for significantly intense reflections: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No