Information card for entry 4300813

Structure parameters

• Formula: C86 H80 Ag2 B2 Cl4 F8 O4 P4
• Calculated formula: C86 H80 Ag2 B2 Cl4 F8 O4 P4
• Title of publication: Two Organometallic Fragments Inclusioned in a 1,3-Alternate Calix[4]arene Tetraphosphane: Evidence for Transition Metal-Arene Interaction through the Cavity
• Authors of publication: Sanghoon Kim; Jong Seung Kim; Sung Kuk Kim; Il-Hwan Suh; Sang Ook Kang; Jaejung Ko
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1846 - 1851
• a: 18.7622 ± 0.0014 Å
• b: 13.7204 ± 0.001 Å
• c: 32.702 ± 0.002 Å
• α: 90°
• β: 97.978 ± 0.001°
• γ: 90°
• Cell volume: 8336.8 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1388
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1404
• Weighted residual factors for all reflections included in the refinement: 0.1727
• Goodness-of-fit parameter for all reflections included in the refinement: 0.883
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No