Information card for entry 4301175

Structure parameters

• Formula: As8 H40 O65 S Sm2 V14
• Calculated formula: As8 O65 S Sm2 V14
• Title of publication: Discrete Polyoxovanadate Cluster into an Organic Free Metal-Oxide-Based Material: Syntheses, Crystal Structures, and Magnetic Properties of a New Series of Lanthanide Linked-POV Compounds [{Ln(H2O)6}2As8V14O42(SO3)].8H2O (Ln = La3+, Sm3+, and Ce3+)
• Authors of publication: T. Arumuganathan; Samar K. Das
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 496 - 507
• a: 13.416 ± 0.003 Å
• b: 12.259 ± 0.003 Å
• c: 18.251 ± 0.004 Å
• α: 90°
• β: 108.05 ± 0.03°
• γ: 90°
• Cell volume: 2854 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0364
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0832
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No