Information card for entry 4301262

Structure parameters

• Formula: C18 H66 Cs9 O95 P2 Sb3 W18
• Calculated formula: C14.8 H11.8 Cs5.5 O83 P2 Sb3 W18
• Title of publication: Organoantimony-Containing Polyoxometalate: [{PhSbOH}3(A-α-PW9O34)2]9-
• Authors of publication: Luis F. Piedra-Garza; Michael H. Dickman; Ovidiu Moldovan; Hans Joachim Breunig; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 411 - 413
• a: 33.899 ± 0.002 Å
• b: 13.6814 ± 0.0009 Å
• c: 21.6122 ± 0.0013 Å
• α: 90°
• β: 103.999 ± 0.003°
• γ: 90°
• Cell volume: 9725.7 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0972
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for significantly intense reflections: 0.1476
• Weighted residual factors for all reflections included in the refinement: 0.1741
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No