Information card for entry 4301405

Structure parameters

• Chemical name: Tetrachloro-1κ,2κ,3κ,4κ-μ(1,2-Bis(1,3-di-tert-butyl-4- tert-butylamino[1,3,2,4]diazadiphosphetidin-2-oxy)ethane-1κ P:2κP':3κP":4κP'")tetragold(I)
• Formula: C53 H122 Au8 Cl10 N12 O4 P8
• Calculated formula: C53 H122 Au8 Cl10 N12 O4 P8
• Title of publication: An Acyclic Dimer of Cyclodiphosphazane {tBuHN(tBuNP)2OCH2}2 Containing Alkoxo and Amido Functionalities: Synthesis, Derivatization, Bi- (PdII, RhI), and Tetranuclear (PdII, AuI, RhIAuI) Transition Metal Complexes
• Authors of publication: Maravanji S. Balakrishna; Ramalingam Venkateswaran; Joel T. Mague
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 1398 - 1406
• a: 9.783 ± 0.001 Å
• b: 18.779 ± 0.002 Å
• c: 14.044 ± 0.002 Å
• α: 90°
• β: 104.775 ± 0.002°
• γ: 90°
• Cell volume: 2494.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1052
• Weighted residual factors for all reflections included in the refinement: 0.1094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No